淡江大學機構典藏:Item 987654321/50482
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    題名: Regeneration of Spent-NaBH4 Back to NaBH4 by Using High-Energy Ball Milling
    作者: Hsueh, Chan-li;Liu, Cheng-hong;Chen, Bing-hung;Chen, Chuh-yung;Kuo, Yi-chia;黃國楨;Hwang, Kuo-jen;Ku, Jie-ren
    貢獻者: 淡江大學化學工程與材料工程學系
    關鍵詞: Sodium borohydride;Sodium metaborate;Magnesium hydride;Yield
    日期: 2009-02-01
    上傳時間: 2010-08-09 18:17:00 (UTC+8)
    出版者: Elsevier
    摘要: High-energy ball milling was employed to regenerate spent-sodium borohydride, i.e., mainly the sodium metaborate (NaBO2), back to sodium borohydride (NaBH4) by a reaction with magnesium hydride (MgH2). The samples were characterized using scanning electron microscopy (SEM), Fourier transform infrared-attenuated total reflectance (FTIR-ATR) spectroscopy, X-ray diffraction (XRD) and nuclear magnetic resonance (NMR) spectroscopy. In general, as the ball-milling duration increases, the yield of NaBH4 increases accordingly and leads to an extreme value of 76%, when MgH2 in stoichiometric excess by 40% was initially present in ball mills.
    關聯: International Journal of Hydrogen Energy 34(4), pp.1717-1725
    DOI: 10.1016/j.ijhydene.2008.12.036
    顯示於類別:[化學工程與材料工程學系暨研究所] 期刊論文

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