淡江大學機構典藏:Item 987654321/50361
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    題名: Microwave-Assisted Base-Catalyzed Cyclization and Nucleophilic Substitution of O-Azidobenzanilides to Synthesize 1,2-Disubstituted Indazol-3-ones
    作者: 蕭永政;Shaw, Arthur Y.;Chen, Yi-ru;Tsai, Chia-hua
    貢獻者: 淡江大學化學學系
    關鍵詞: Base-catalyzed cyclization;indazol-3-one;microwave-assisted
    日期: 2009-01-01
    上傳時間: 2010-08-09 15:51:06 (UTC+8)
    出版者: Taylor & Francis
    摘要: A series of 1,2-disubstituted indazol-3-ones were synthesized by microwave-assisted base-catalyzed cyclization and nucleophilic substitution of o-azidobenzanilides. Among five tested reaction conditions, the cyclization of o-azidobenzanilides catalyzed by sodium hydride in DMF, sequentially followed by the nucleophilic substitution under microwave irradiation, exhibited the optimal results. Moreover, compared to the counterparts prepared by conventional heat, this method demonstrated a more expeditious and efficient process to establish a diversified 1,2-disubstituted indazol-3-one library for high-throughput biological screening.
    關聯: Synthetic Communications 39(15), pp.2647-2663
    DOI: 10.1080/00397910802663386
    顯示於類別:[化學學系暨研究所] 期刊論文

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