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    Please use this identifier to cite or link to this item: http://tkuir.lib.tku.edu.tw:8080/dspace/handle/987654321/25078

    Title: 2, 9-diphenylamino-1, 10-phenanthroline
    Authors: Liu, Hai-yang;Luo,Chi-fong;Chuang, Kuo-shen;王文竹;Wang, Wen-jwu
    Contributors: 淡江大學化學學系
    Date: 2001-05-25
    Issue Date: 2009-12-01
    Publisher: Basel: Molecular Diversity Preservation International (MDPI)
    Abstract: 2,9-Dichloro-1,10-phenanthroline was prepared by a previously published method [1]. 2,9-Dichloro-1,10-phenanthroline (50 mg) was placed in a flask where the temperature was raised 150 °C with oil-bath,
    and aniline was introduced under N2 gas. The temperature was raised to 250 °C and maintained for 5 hours. The mixture was purified by recrystalization from methanol, to give 2,9-diphenylamino-1,10 phenanthroline as a dark brown crystal (30 mg, yield: 30.0%).
    Relation: Molecules 6(6), pp.M230
    DOI: 10.3390/M230
    Appears in Collections:[Graduate Institute & Department of Chemistry] Journal Article

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