Synthesis and characterization of MSU-2 synthesized by using tetraethylorthosilicate and Triton X-100

doi:10.1088/1757-899X/736/4/042026

淡江大學機構典藏 > 工學院 > 化學工程與材料工程學系暨研究所 > 期刊論文 > Item 987654321/120934

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题名:	Synthesis and characterization of MSU-2 synthesized by using tetraethylorthosilicate and Triton X-100
作者:	Lee, X Y;Chew, T L;Oh, P C;Jawad, Z A;Ho, C D
日期:	2019-10
上传时间:	2021-08-18 12:13:33 (UTC+8)
摘要:	Adsorption technology is one of the well-established gas separation techniques as it can minimize cost and energy requirement for CO2 separation. Mesoporous silicas such as MSU-2 appears to be a good adsorbent as it comprises of three-dimensional (3D) wormhole framework structures that are highly interconnected which minimize the diffusion resistance of CO2 through its pore structure. Current study focus on the preparation of MSU-2 and investigation on the CO2 adsorption on the synthesized MSU-2. In this study, MSU-2 was prepared by using tetraethylorthosilica (TEOS) as a source of silica in the presence of non- ionic polyethyleneoxide (PEO)-based surfactants under an acidic condition where the pH is 2 at 55 °C for 48 hours via the fluoride-assisted two-step synthesis process. The two main steps involved are hydrolysis of TEOS and condensation of silica. The morphology, crystallinity, functional groups and pore characteristics of MSU-2 were investigated by using characterization method of Field Emission Scanning Electron Microscope (FESEM), Energy Dispersive X-Ray (EDX) Spectrometry, X-ray Diffractometer (XRD), Fourier Transform Infrared Spectroscopy (FTIR) and Brunauer-Emmett-Teller (BET). The synthesized MSU-2 was well crystallized and possessed a uniform monodisperse microspherical morphology with BET surface area, pore volume and pore size of 964 m2/g, 0.98 cm3/g and 4.1 nm, respectively. All the characterization results showed that MSU-2 was successfully synthesized via solution precipitation method. In conclusion, the high BET surface area of the synthesized MSU-2 shows that MSU-2 is a very potential candidate as a good adsorbent for gases.
關聯:	IOP Conf. Series: Materials Science and Engineering, 736 (2020) 042026
DOI:	10.1088/1757-899X/736/4/042026
显示于类别:	[化學工程與材料工程學系暨研究所] 期刊論文

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